All pollutant analyses, including sampling techniques, to be submitted as part of
a wastewater discharge permit application or report shall be performed in accordance
with the techniques prescribed in 40 CFR Part 136, and Chapter 62-160, F.A.C. unless
otherwise specified in an applicable categorical pretreatment standard. If 40 CFR
part 136 does not contain sampling or analytical techniques for the pollutant in question,
sampling and analyses must be performed in accordance with procedures approved by
EPA and the FDEP.